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Folders: ROOT > ScienceBase Catalog > USGS Data Release Products > Silicified wood from around Old Faithful Geyser, Yellowstone National Park ( Show all descendants )

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___Silicified wood from around Old Faithful Geyser, Yellowstone National Park
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Radiocarbon dating of silicified wood was performed at the U.S. Geological Survey’s Radiocarbon Laboratory in Denver, Colorado. All samples were chemically treated using the standard acid-base-acid (ABA) procedure before being combusted online in the presence of excess high-purity oxygen. Water and other contaminant gases were removed using cryogenic separation techniques, and the resulting purified CO2 gas was measured manometrically and converted to graphite using an iron catalyst and hydrogen reduction (Vogel et al., 1984). Graphite targets were then submitted for accelerator mass spectrometry 14C analysis at the National Ocean Sciences Accelerator Mass Spectrometry facility in Woods Hole, Massachusetts. All...
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Silicified wood samples were vacuum impregnated with epoxy, sectioned, and sputter coated with 10 nm Au/Pd at the U.S. Geological Survey, Menlo Park, CA. Samples were imaged in a Tescan VEGA3 Scanning Electron Microscope (SEM) equipped with an Oxford 150 mm2 X-MaxN large area energy dispersive spectrometer at the U.S. Geological Survey, Menlo Park, CA. Backscatter (BSE) images were collected with an accelerating voltage (HV) of 30 kV and a working distance (WD) of ~15 mm. Magnification is indicated on individual images. The data files for Scanning Electron Microsocopy (SEM) contain representative SEM-BSE images of samples OFL101 and OFL103-2. This research was conducted under Yellowstone Research Permit YELL-SCI-8030.


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