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The U.S. Geological Survey (USGS) in cooperation with the California State Water Resources Control Board collected produced water samples for analysis of volatile organic compounds (VOCs) in the eight California oil fields of Fruitvale, Lost Hills, North Belridge, Orcutt, Placerita, South Belridge, Midway-Sunset, and Buena Vista from 2016 to 2020. Sampled sites included oil wells; injectate from tanks, pipelines, and injection wells where produced water from many wells, after removal of oil, is stored or transported prior to underground injection; integrated produced water from many oil wells collected from pipelines before oil removal; and surface disposal ponds where produced water, after removal of oil, is disposed...
The Bemidji crude oil spill site is a long-term USGS study site to understand the fate of crude oil in the shallow subsurface. A description of the site can be found at https://mn.water.usgs.gov/projects/bemidji. In 2014 concentrations of non-volatile dissolved organic carbon (NVDOC) were three times higher than diesel range organics (DRO) in the contaminant plume*. This is important because most of the NVDOC in the plume is composed of partial transformation products of compounds from the crude oil that are not reflected in a DRO analysis. In 2016 we conducted a campaign to determine if DRO values continue to reflect only a fraction of the NVDOC. These data are the results of that campaign. A total of 25 wells...
Categories: Data;
Tags: USGS Science Data Catalog (SDC)
The dataset consists of 30-year percentage depletion calculations, hydrocarbon group compositions, organic carbon mass fractions and hydrocarbon concentrations for 16 locations sampled at the Bemidji (MN) oil spill study site. Also included in the dataset are concentrations for 33 individual volatile hydrocarbons from the aforementioned sampling locations.
The U.S. Geological Survey (USGS) in cooperation with the California State Water Resources Control Board collected produced water and gas samples in the Midway-Sunset, Poso Creek, and Buena Vista Oil Fields in Kern County in 2020 and 2021. Sampled sites included oil wells; injectate from tanks, pipelines, and injection wells where produced water from many wells, after removal of oil, is stored or transported prior to underground injection; and integrated produced water from many oil wells collected from pipelines before oil removal. This digital dataset contains the site information, analyzing laboratories and methods, and water and gas chemistry and quality-control results for these samples. Chemistry results include...
In a crude-oil-contaminated sandy aquifer at the Bemidji site in northern Minnesota, biodegradation of petroleum hydrocarbons resulted in transient increases in magnetic susceptibility under high water table conditions. The magnetic susceptibility subsequently decreased again when the water table dropped. This data set was assembled to illustrate the cause of the magnetic susceptibility changes. These data show that alkalinity is high and dissolved oxygen is low in the area where the increased magnetic susceptibility is found. The decrease in the magnetic susceptibility can be attributed to the long term decline in sediment Fe(III) concentrations with time. The decrease is caused by iron reducing bacteria converting...
Categories: Data;
Tags: Bemidji,
Pinewood,
USGS Science Data Catalog (SDC),
dissolved metals,
groundwater quality,
Note: this version has been superseded by version 3.0: Trost, J.J., Krall, A.L., Baedecker, M., Cozzarelli, I.M., Herkelrath, W.N., Jaeschke, J.B., Delin, G.N., Berg, A.M., and Bekins, B.A., 2020, Data Sets from the National Crude Oil Spill Fate and Natural Attenuation Research Site near Bemidji, Minnesota, USA (ver. 3.0, March 2020): U.S. Geological Survey data release, https://doi.org/10.5066/P9FJ8I0P. This U.S. Geological Survey (USGS) Data Release provides analytical data from samples and measurements completed at the National Crude Oil Spill Fate and Natural Attenuation Research Site near Bemidji, Minnesota (Site) between 1984 and 2010. Included are inorganic and organic chemistry data from water, oil, and...
The Marcellus Shale Energy and Environment Laboratory (MSEEL) site is a long-term field site and laboratory at the Northeast Natural Energy LLC (NNE) production facility, adjacent to the Monongahela River, located in western Monongalia County, West Virginia, USA. NNE began drilling two horizontal production wells, MIP (Morgantown Industrial Park) -5H and MIP-3H, in the Marcellus Shale in 2014. The wells were completed in December 2015. Large volumes of wastewater are generated with natural gas production. These wastewaters contain organic and inorganic chemical constituents from fracturing fluids used during drilling and stimulation of gas in host rocks/shale, as well as chemical compounds that are derived from...
This U.S. Geological Survey (USGS) Data Release is focused on the geochemistry of wastewater (including flowback and produced water) samples, co-produced with natural gas, collected from the Marcellus Shale Energy and Environment Laboratory (MSEEL) site. MSEEL is a long-term field site and laboratory at the Northeast Natural Energy LLC (NNE) production facility, adjacent to the Monongahela River, located in western Monongalia County, West Virginia, USA. NNE began drilling two horizontal production wells, MIP (Morgantown Industrial Park) -5H and MIP-3H, in the Marcellus Shale in 2014. The wells were completed in December 2015. Large volumes of wastewater are generated with natural gas production. These wastewaters...
In crude-oil-contaminant plumes the dissolved organic carbon (DOC) is mainly hydrocarbon degradation intermediates only partly quantified by the diesel range total petroleum hydrocarbon (TPHd) method. To understand potential biological effects of degradation intermediates we tested three fractions of DOC: (1) solid phase extract (HLB); (2) dichloromethane (DCM-total) extract used in TPHd; and (3) DCM extract with hydrocarbons isolated by silica gel cleanup (DCM-SGC). Bioactivity of extracts from five wells spanning a range of DOC was tested using an in vitro multiplex reporter system that evaluates modulation of activity of 46 transcription factors; extracts were evaluated at concentrations equivalent to the well...
Data supporting "Common hydraulic fracturing fluid additives alter the structure and function of anaerobic microbial communities", describing iron reduction experiments, microbial community profiling, and statistical testing of data.
Categories: Data;
Tags: Aquatic Biology,
Ecology,
Energy Resources,
Environmental Health,
Fayette County,
Management of petroleum-impacted waters by monitored natural attenuation (MNA) requires an understanding of the toxicology of both the original compounds released as well as the transformation products formed during natural breakdown. Here, we report data from a groundwater plume consisting of a mixture of crude oil compounds and transformation products resulting from a crude-oil release in August, 1979 near Bemidji, MN, USA. Water samples were characterized for activation of 52 human nuclear receptor (NR) activities and 50 transcriptional pathways associated with toxic responses. Five replicate analyses were performed for each solution at strengths of 1, 3, and 10 times the sample concentration. Radar plots of...
Categories: Data;
Tags: Bemidji,
Pinewood,
USGS Science Data Catalog (SDC),
Water Quality,
groundwater quality,
Note: This data release is temporarily unavailable.
These analyses provide the basic geochemical composition of urban stormwater runoff from rainwater/stormwater that does or has the potential to infiltrate groundwater from Green Infrastructure control measures. These measures are able to mimic the natural landscape with engineered designed systems to enhance stormwater infiltration to groundwater.
Categories: Data;
Tags: Geochemistry,
USGS Science Data Catalog (SDC),
Water Quality,
alkalinity,
anions,
This U.S. Geological Survey (USGS) Data Release is focused on the geochemistry of wells within the oil zone and groundwater monitoring wells away from the oiled zone at the National Crude Oil Spill Fate and Natural Attenuation Research Site, Bemidji MN (USA) from 1985-2015. The site located in Beltrami County is where a high-pressure pipeline carrying crude oil burst in 1979 and spilled approximately 1.7 million liters (10,700 barrels) of crude oil into glacial outwash deposits. Researchers and scientists from government agencies, academic institutions, the regulatory community, and private companies have conducted extensive investigations of groundwater geochemistry in hopes of understanding the evolution of plumes...
Groundwater samples were collected in June 2018 from a background (reference) well located 200 m upgradient from the source and five wells along a flowline in the plume at 39, 68, 102, 125, and 254 m downgradient from the source. Before sampling, at least three times the water volume in the well casing was purged and field parameters (temperature, dissolved oxygen, specific conductance, and pH) were stable. Two samples from each well were collected into unpreserved 1 L amber bottles and shipped on ice overnight to a commercial lab. The two samples were extracted using dichloromethane (DCM; EPA Method 3510). One sample extract was treated with silica gel cleanup (SGC) column (USEPA method 3630C). Aliquots of the...
This data describes the relative luminescence units (RLUs) and relative fluorescence units (RFUs) of lysates of aryl-hydrocarbon responsive chemically-activated luciferase expression human hepatoma HG2L7.5c1 cells which were exposed for 4 or 24 h to beta-naphthoflavone dilutions, 2,3,7,8-tetrachlorodibenzo-p-dioxin dilutions, or dilutions of groundwater extracts collected from wells within or near an oil-contaminated area. This data also describes RFUs of bovine serum albumin standards which were used to convert the RFUs of the cell lysates to protein with which to normalize the RLUs of the cell lysates.
In a crude-oil-contaminated sandy aquifer at the Bemidji site in northern Minnesota, biodegradation of petroleum hydrocarbons has resulted in release of naturally occurring As to groundwater under Fe-reducing conditions. This data set was collected for a study that used chemical extractions of aquifer sediments collected in 1993 and 2011-2014 to evaluate the relationship between Fe and As in different redox zones (oxic, methanogenic, Fe-reducing, anoxic-sub-oxic transition) of the contaminated aquifer over a twenty year period. The data presented showed that 1) the aquifer has the capacity to naturally attenuate the plume of dissolved As, primarily through sorption; 2) Fe and As are linearly correlated in sediment...
Categories: Data;
Tags: USGS Science Data Catalog (SDC),
Water Quality,
arsenic,
biodegradation,
biogeochemical cycling,
This U.S. Geological Survey (USGS) Data Release provides concentrations from groundwater and soil extracts for iron (Fe), barium (Ba), strontium (Sr), cobalt (Co), and nickel (Ni). Groundwater analyses for pH and alkalinity are also included. Samples were collected at the National Crude Oil Spill Fate and Natural Attenuation Research Site, near Bemidji MN (USA) between 2009-2019. The site is in Beltrami County, where a high-pressure pipeline carrying crude oil burst in 1979 and spilled approximately 1.7 million liters (10,700 barrels) into glacial outwash deposits. A trace element plume occurred at the site, in which concentrations of Fe, Co, Ni, Ba, and Sr were mobilized from the sediments into the groundwater....
A large spill of wastewater from oil and gas operations was discovered adjacent to Blacktail Creek near Williston, North Dakota in January 2015. To determine the effects of this spill on streambed microbial communities over time, bed sediment samples were taken from Blacktail Creek upstream, adjacent to, and at several locations downstream from the spill site. Blacktail Creek is a tributary of the Little Muddy River, and additional samples were taken upstream and downstream from the confluence of Blacktail Creek and the Little Muddy River. Samples were collected in February 2015, June 2015, June 2016, and June 2017. DNA was extracted from these sediments, and sequencing of the 16S ribosomal RNA gene was performed...
Categories: Data;
Tags: Aquatic Biology,
Blacktail Creek,
DNA sequencing,
Ecology,
Little Muddy River,
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